Acetylenic ethers from alcohols and their reduction to Z- and E-enol ethers: preparation of 1-menthoxy-1-butyne from menthol and conversion to (Z)- and (E)-1-menthoxy-1-butene
CAS index name: [Cyclohexane, 2-(1-butynyloxy)-4-methyl-1-(1-methylethyl)-[1S-(1α,2β,4β)]-], and [[[Cyclohexane, 2-(1-butenyloxy)-4-methyl-1-(1-methylethyl)-, [1S-[1α,2β(Z),4β]]- and [1S-[1α,2β(E),4β]]-
Organic SynthesesReduction
A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.
Reagents
The compound this preparation makes is not in the catalogue, so no reagents or figures are listed here.
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- Apparatus for catalytic reduction
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