Aldehydes from acid chlorides by reduction of ester-mesylates with sodium borohydride: cyclobutanecarboxaldehyde

Organic SynthesesReduction

Reaction scheme of Aldehydes from acid chlorides by reduction of ester-mesylates with sodium borohydride: cyclobutanecarboxaldehyde from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 6, p. 312; Vol. 51, p. 11.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
Cyclobutanecarboxaldehyde2987-17-9 · C5H8O product — 84.12 — Irritant (GHS07)Warning

Search the literature