Organic Syntheses procedures

2,353–2,376 of 2,861

1. Radical allylation of B-alkylcatecholboranes Org. Synth. Vol. 83, p. 24 · Darmency et al.
2. Radical anion arylation: diethyl phenylphosphonate Org. Synth. Coll. Vol. 6, p. 451; Vol. 58, p. 134 · Bunnett and Weiss
3. Reaction of aryl halides with π-allylnickel halides: methallylbenzene Org. Synth. Coll. Vol. 6, p. 722; Vol. 52, p. 115 · Semmelhack and Helquist
4. Reaction of sulfoxides with diethylaminosulfur trifluoride: fluoromethyl phenyl sulfone, a reagent for the synthesis of fluoroalkenes Org. Synth. Coll. Vol. 9, p. 446; Vol. 72, p. 209 · McCarthy et al.
5. Reagent for Divalent Sulfur Protection: Preparation of 4-Methylbenzenesulfonothioic Acid, S-[[[(1,1-Dimethylethyl)-Dimethylsilyl]oxy]methyl] EsterProtection Org. Synth. Vol. 90, p. 10 · Wang and Clive
6. Reagents for synthesis of organoselenium compounds: diphenyl diselenide and benzeneselenenyl chloride Org. Synth. Coll. Vol. 6, p. 533; Vol. 59, p. 141 · Reich et al.
7. Rearrangement of 4-aryl-4-hydroxy-2,3-dialkoxycyclobutenones to annulated hydroquinones and quinones: 5,6-diethoxybenzofuran-4,7-dioneRearrangement Org. Synth. Coll. Vol. 8, p. 179; Vol. 69, p. 220 · Perri et al.
8. Rearrangement of bridgehead alcohols to polycyclic ketones by fragmentation-cyclization: 4-protoadamantanone (tricyclo-[4.3.1.03,8]decan-4-one)Rearrangement Org. Synth. Coll. Vol. 6, p. 958; Vol. 59, p. 147 · Majerski and Hamersak
9. Rearrangement of trans-stilbene oxide to diphenylacetaldehyde with catalytic methylaluminum bis(4-bromo-2,6-di-tert-butylphenoxide)Rearrangement Org. Synth. Coll. Vol. 9, p. 356; Vol. 72, p. 95 · Ooi et al.
10. Reduction of alkyl halides and tosylates with sodium cyanoborohydride in hexamethylphosphoric triamide (HMPA):A. 1-Iododecane to n-decaneb. 1-Dodecyl tosylate to n-dodecaneReduction Org. Synth. Coll. Vol. 6, p. 376; Vol. 53, p. 107 · Hutchins et al.
11. Reduction of carboxylic acids to aldehydes: 6-oxodecanalReduction Org. Synth. Coll. Vol. 8, p. 498; Vol. 66, p. 121 · Fujisawa and Sato
12. Reduction of conjugated alkenes with chromium(II) sulfate: diethyl succinateReduction Org. Synth. Coll. Vol. 5, p. 993; Vol. 49, p. 98 · Zurqiyah and Castro
13. Reduction of ketones by use of the tosylhydrazone derivatives: androstan-17 β-olReduction Org. Synth. Coll. Vol. 6, p. 62; Vol. 52, p. 122 · Caglioti
14. Reduction of ketones to hydrocarbons with triethylsilane: m-nitroethylbenzeneReduction Org. Synth. Coll. Vol. 7, p. 393; Vol. 60, p. 108 · Fry et al.
15. Reduction of organic halides. Chlorobenzene to benzeneReduction Org. Synth. Coll. Vol. 5, p. 998; Vol. 47, p. 103 · Bryce-Smith and Wakefield
16. Reduction of quinones with hydriodic acid: benz[a]anthraceneReduction Org. Synth. Coll. Vol. 7, p. 18; Vol. 62, p. 165 · Konieczny and Harvey
17. Reduction of sulfonyl halides with zinc powder: S-methyl methanethiosulfonateReduction Org. Synth. Vol. 78, p. 99 · Chemla and Karoyan
18. Reduction of α-amino acids: L-valinolReduction Org. Synth. Coll. Vol. 7, p. 530; Vol. 63, p. 136 · Dickman et al.
19. Reductive amination with sodium cyanoborohydride: N,N-dimethylcyclohexylamine Org. Synth. Coll. Vol. 6, p. 499; Vol. 52, p. 124 · Borch
20. Reductive annulation of vinyl sulfones: bicyclo[4.3.0.]non-1-en-4-oneCyclization Org. Synth. Coll. Vol. 8, p. 38; Vol. 67, p. 163 · Lin and Paquette
21. Reductive arylation of electron-deficient olefins: 4-(4-chlorophenyl)butan-2-one Org. Synth. Coll. Vol. 7, p. 105; Vol. 62, p. 67 · Citterio
22. Reductive cleavage of allylic alcohols, ethers, or acetates to olefins: 3-methylcyclohexene Org. Synth. Coll. Vol. 6, p. 769; Vol. 56, p. 101 · Elphimoff-Felkin and Sarda
23. Reductive cleavage of vinyl phosphorodiamidates: 17β-tert-butoxy-Gα-androst-2-ene Org. Synth. Coll. Vol. 7, p. 66; Vol. 61, p. 116 · Ireland et al.
24. Reductive coupling of carbonyls to alkenes: adamantylideneadamantaneCross-coupling Org. Synth. Coll. Vol. 7, p. 1; Vol. 60, p. 113 · Fleming and McMurry