Organic Syntheses procedures

2,545–2,568 of 2,861

1. Synthesis of alpha-halo ethers from symmetric acetals and in situ methoxymethylation of an alcohol Org. Synth. Vol. 84, p. 102 · Berliner and Belecki
2. Synthesis of amino acid ester isocyanates: methyl (S)-2-isocyanato-3-phenylpropanoate Org. Synth. Vol. 78, p. 220 · Tsai et al.
3. Synthesis of aminoarenethiolato-copper(I) complexes Org. Synth. Vol. 85, p. 209 · Sperotto et al.
4. Synthesis of an anti-α-amino epoxide by one-carbon homologation of an α-amino ester: ((2S,3S)-1,2-epoxy-3-(BOC-amino)-4-phenylbutane) Org. Synth. Vol. 84, p. 58 · Wanga and Nugent.b
5. Synthesis of an N-substituted lactam using an intramolecular Schmidt reaction: formation of 2,3,11,11a-tetrahydro-1H-benzo[d]pyrrolo[1,2-a]azepin-5(6H)-oneRearrangement Org. Synth. Vol. 84, p. 347 · Grecian and Aubé
6. Synthesis of Arylboronic Pinacol Esters from Corresponding ArylaminesRearrangement Org. Synth. Vol. 91, p. 106 · Qiu et al.
7. Synthesis of biaryls via palladium-catalyzed cross-coupling: 2-methyl-4'-nitrobiphenylCross-coupling Org. Synth. Coll. Vol. 8, p. 430; Vol. 66, p. 67 · Negishi et al.
8. Synthesis of chiral (E)-crotylsilanes: [3R- and 3S-]-(4E)-methyl 3-(dimethylphenylsilyl)-4-hexenoate Org. Synth. Vol. 75, p. 78 · Beresis et al.
9. Synthesis of chiral non-racemic diols from (S,S)-1,2,3,4-diepoxybutane: (2S,3S)-dihydroxy-1,4-diphenylbutane Org. Synth. Vol. 76, p. 101 · Robbins et al.
10. Synthesis of chiral pyridine bis(oxazoline) ligands for nickel-catalyzed asymmetric Negishi cross-couplings of secondary allylic chlorides with alkylzincs: 2,6-bis[(4R)-4,5-dihydro-4- (2-phenylethyl)-2-oxazolyl]- pyridineCross-coupling Org. Synth. Vol. 87, p. 310 · Lou and Fu
11. Synthesis of cis-4a(S),8a(R)-perhydro-6(2H)-isoquinolinones from quinine: 4a(S), 8a(R)-2-benzoyloctahydro-6(2H)-isoquinolinone Org. Synth. Vol. 75, p. 223 · Hutchison et al.
12. Synthesis of cyclobutanones via 1-bromo-1-ethoxycyclopropane: (E)-2-(1-propenyl)cyclobutanone Org. Synth. Coll. Vol. 8, p. 556; Vol. 67, p. 210 · Miller and Gadwood
13. Synthesis of Cyclobutarenes by Palladium-Catalyzed C(sp3)-H Bond Arylation: Preparation of Methyl 7-Methylbicyclo[4.2.0]Octa-1,3,5-Triene-7-Carboxylate Org. Synth. Vol. 89, p. 510 · Davi et al.
14. Synthesis of dimethyl 2-phenylcyclopropane-1,1-dicarboxylate using an iodonium ylide derived from dimethyl malonate Org. Synth. Vol. 87, p. 115 · Goudreau et al.
15. Synthesis of dithieno[3,2-b:2',3'-d]thiophene Org. Synth. Vol. 83, p. 209 · Frey et al.
16. Synthesis of electron-deficient secondary phosphine oxides and secondary phosphines: bis[3,5-bis(trifluoromethyl)phenyl]phosphine oxide and bis[3,5-bis(trifluoromethyl)phenyl]phosphine Org. Synth. Vol. 84, p. 242 · Busacca et al.
17. Synthesis of enamides from ketones: preparation of N-(3,4-dihydronaphthalene-1-yl)acetamide Org. Synth. Vol. 87, p. 275 · Zhao et al.
18. Synthesis of enantiopure di(tert-butyl) (2S,4S)-4-hydroxy-6-oxo-1,2-piperidinedicarboxylate. A useful building block for the preparation of 4-hydroxypipecolate derivatives Org. Synth. Vol. 85, p. 147 · Chaloin et al.
19. Synthesis of epoxides using dimethyldioxirane: trans-stilbene oxide Org. Synth. Coll. Vol. 9, p. 288; Vol. 74, p. 91 · Murray and Singh
20. Synthesis of Et2SBr•SbCl5Br and its use in biomimetic brominative polyene cyclizationsCyclization Org. Synth. Vol. 88, p. 54 · Snyder and Treitler
21. Synthesis of ethyl 2-ethanoyl-2-methyl-3-phenylbut-3-enoate Org. Synth. Vol. 86, p. 325 · Fujimoto et al.
22. Synthesis of functionalized enynes by palladium/copper-catalyzed coupling reactions of acetylenes with (Z)-2,3-dibromopropenoic acid ethyl ester: (Z)-2-bromo-5-(trimethylsilyl)-2-penten-4-ynoic acid ethyl esterCross-coupling Org. Synth. Coll. Vol. 9, p. 117; Vol. 72, p. 104 · Myers and Dragovich
23. Synthesis of furans via rhodium(II) acetate-catalyzed reaction of acetylenes with α-diazocarbonyls: ethyl 2-methyl-5-phenyl-3-furancarboxylate Org. Synth. Coll. Vol. 9, p. 422; Vol. 70, p. 93 · Davies et al.
24. Synthesis of Highly Enantiomerically Enriched Amines by Asymmetric Transfer Hydrogenation of N-(tert-Butylsulfinyl)IminesReduction Org. Synth. Vol. 90, p. 338 · Guijarro et al.