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LIPASE-CATALYZED RESOLUTION OF 4-TRIMETHYLSILYL-3-BUTYN-2-OL AND CONVERSION OF THE (R)-ENANTIOMER TO (R)-3-BUTYN-2-YL MESYLATE AND (P)-1-TRIBUTYLSTANNYL-1,2-BUTADIENE (3-Butyn-2-ol, 4-(trimethylsilyl)-, (2R)- and Stannane, 1,2-butadienyltributyl-, (P)-)

Reactions · Organic Syntheses

LIPASE-CATALYZED RESOLUTION OF 4-TRIMETHYLSILYL-3-BUTYN-2-OL AND CONVERSION OF THE (R)-ENANTIOMER TO (R)-3-BUTYN-2-YL MESYLATE AND (P)-1-TRIBUTYLSTANNYL-1,2-BUTADIENE (3-Butyn-2-ol, 4-(trimethylsilyl)-, (2R)- and Stannane, 1,2-butadienyltributyl-, (P)-)

Reaction equation for LIPASE-CATALYZED RESOLUTION OF 4-TRIMETHYLSILYL-3-BUTYN-2-OL AND CONVERSION OF THE (R)-ENANTIOMER TO (R)-3-BUTYN-2-YL MESYLATE AND (P)-1-TRIBUTYLSTANNYL-1,2-BUTADIENE (3-Butyn-2-ol, 4-(trimethylsilyl)-, (2R)- and Stannane, 1,2-butadienyltributyl-, (P)-)

Preparation of 3-Butyn-2-ol, 4-(trimethylsilyl)-, (2R)- and Stannane, 1,2-butadienyltributyl-, (P)-. Submitted by James A. Marshall and Harry Chobanian1. DOI: 10.15227/orgsyn.082.0043.

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