Formyl transfer to Grignard reagents with N-formylpiperidine: 3-phenylpropionaldehyde
Organic SynthesesOrganometallic addition

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.
Reagents
| Compound | Role | Equiv | MW (g/mol) | ρ (g/mL) | Safety |
|---|---|---|---|---|---|
| Hydrocinnamaldehyde104-53-0 · C9H10O | product | — | 134.18 | — | Warning |
Named reactions in this procedure
More organometallic addition reactions
- Aldehydes from 4,4-dimethyl-2-oxazoline and Grignard reagents: o-anisaldehyde
- Cross-Coupling of Alkenyl/Aryl Carboxylates with Grignard Reagents via Fe-Catalyzed C-O Bond Activation
- Highly reactive magnesium for the preparation of Grignard reagents: 1-norbornanecarboxylic acid
- Iron-Catalyzed Selective Conjugate Addition of Aryl Grignard Reagents to 2,4-Alkadienoates: tert-Butyl (Z)-5-Phenyl-3-hexenoate
- Ketones from carboxylic acids and Grignard reagents: methyl 6-oxodecanoate
- Nickel-catalyzed coupling of aryl O-carbamates with Grignard reagents: 2,7-dimethylnaphthalene