Alkynes via phase transfer–catalyzed dehydrohalogenation: propiolaldehyde diethyl acetal

CAS index name: 1-Propyne, 3,3-diethoxy-

Organic SynthesesHalogenation

Reaction scheme of Alkynes via phase transfer–catalyzed dehydrohalogenation: propiolaldehyde diethyl acetal from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 6, p. 954; Vol. 59, p. 10.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
3,3-Diethoxy-1-propyne10160-87-9 · C7H12O2 product — 128.17 — Flammable (GHS02)Irritant (GHS07)Warning

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