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2861 reactions imported from Wikipedia named-reactions and Organic Syntheses archives. Filter by source or search by name + summary.

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Equation Name Summary Source
SYNTHESIS OF SUBSTITUTED INDAZOLES VIA [3+2] CYCLOADDITION OF BENZYNE AND DIAZO COMPOUNDS (1H-indazole-3-carboxylic acid, ethyl ester) Cycloaddition Preparation of 1H-indazole-3-carboxylic acid, ethyl ester. Submitted by Feng Shi and Richard C. Larock1. DOI: 10.15227/orgsyn.087.0095. Organic Syntheses
SYNTHESIS OF SYMMETRICAL trans -STILBENES BY A DOUBLE HECK REACTION OF (ARYLAZO)AMINES WITH VINYLTRIETHOXYSILANE: trans-4,4'-DIBROMOSTILBENE (Benzene, 1,1'-(1,2-ethenediyl)bis[4-bromo-, (E)- using Silane, ethenyltriethoxy-) Cross-coupling Preparation of Benzene, 1,1'-(1,2-ethenediyl)bis[4-bromo-, (E)- using Silane, ethenyltriethoxy-. Submitted by Saumitra Sengupta and Subir K. Sadhukhan1. DOI: 10.15227/orgsyn.079.0052. Organic Syntheses
SYNTHESIS OF TERMINAL 1,3-DIYNES VIA SONOGASHIRA COUPLING OF VINYLIDENE CHLORIDE FOLLOWED BY ELIMINATION. PREPARATION OF 1,3-DECADIYNE Cross-coupling Preparation of SYNTHESIS OF TERMINAL 1,3-DIYNES VIA SONOGASHIRA COUPLING OF VINYLIDENE CHLORIDE FOLLOWED BY ELIMINATION. PREPARATION OF 1,3-DECADIYNE. Submitted by Amanda L. Kohnen and Rick L. Danheis… Organic Syntheses
SYNTHESIS OF TERT-BUTYL (1S,2S)-2-METHYL-3-OXO-1-PHENYLPROPYLCARBAMATE BY ASYMMETRIC MANNICH REACTION Addition Preparation of SYNTHESIS OF TERT-BUTYL (1S,2S)-2-METHYL-3-OXO-1-PHENYLPROPYLCARBAMATE BY ASYMMETRIC MANNICH REACTION. Submitted by Jung Woon Yang, Subhas Chandra Pan, and Benjamin List1. DOI: 10.15227… Organic Syntheses
SYNTHESIS OF TETRAORGANOSILANES: (CHLOROMETHYL)DIMETHYLPHENYLSILANE Preparation of SYNTHESIS OF TETRAORGANOSILANES: (CHLOROMETHYL)DIMETHYLPHENYLSILANE. Submitted by Kei Murakami, Hideki Yorimitsu, and Koichiro Oshima1. DOI: 10.15227/orgsyn.087.0178. Organic Syntheses
Synthesis of Tetrasubstituted 1H-Pyrazoles by Copper-mediated Coupling of Enaminones with Nitriles Cross-coupling Preparation of Synthesis of Tetrasubstituted 1H-Pyrazoles by Copper-mediated Coupling of Enaminones with Nitriles. Submitted by Mamta Suri and Frank Glorius*1. DOI: 10.15227/orgsyn.091.0211. Organic Syntheses
Synthesis of Trifluoromethyl Ketones from Carboxylic Acids: 4-(3,4-Dibromophenyl)-1,1,1-trifluoro-4-methylpentan-2-one Preparation of Synthesis of Trifluoromethyl Ketones from Carboxylic Acids: 4-(3,4-Dibromophenyl)-1,1,1-trifluoro-4-methylpentan-2-one. Submitted by Jonathan T. Reeves1, Zhulin Tan, Daniel R. Fandrick,… Organic Syntheses
SYNTHESIS OF TRIS(2-PERFLUOROHEXYLETHYL)TIN HYDRIDE: A HIGHLY FLUORINATED TIN HYDRIDE WITH ADVANTAGEOUS FEATURES OF EASY PURIFICATION (Stannane, tris-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-) Preparation of Stannane, tris-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl)-. Submitted by Aimee Crombie, Sun-Young Kim, Sabine Hadida, and Dennis P. Curran1. DOI: 10.15227/orgsyn.079.0001. Organic Syntheses
SYNTHESIS OF UNSYMMETRICAL BIARYLS USING A MODIFIED SUZUKI CROSS-COUPLING: 4-BIPHENYLCARBOXALDEHYDE ([1,1'-Biphenyl]-4-carboxaldehyde) Cross-coupling Preparation of [1,1'-Biphenyl]-4-carboxaldehyde. Submitted by Bret E. Huff, Thomas M. Koenig, David Mitchell, and Michael A. Staszak1. DOI: 10.15227/orgsyn.075.0053. Organic Syntheses
SYNTHESIS OF YNAMIDES BY COPPER-MEDIATED COUPLING OF 1,1-DIBROMO-1-ALKENES WITH NITROGEN NUCLEOPHILES. PREPARATION OF 4-METHYL-N-(2-PHENYLETHYNYL)-N-(PHENYLMETHYL)BENZENESULFONAMIDE Cross-coupling Preparation of SYNTHESIS OF YNAMIDES BY COPPER-MEDIATED COUPLING OF 1,1-DIBROMO-1-ALKENES WITH NITROGEN NUCLEOPHILES. PREPARATION OF 4-METHYL-N-(2-PHENYLETHYNYL)-N-(PHENYLMETHYL)BENZENESULFONAMIDE. Su… Organic Syntheses
SYNTHESIS OF YNAMIDES BY N-ALKYNYLATION OF AMINE DERIVATIVES. PREPARATION OF N-ALLYL-N-(METHOXYCARBONYL)-1,3-DECADIYNYLAMINE Preparation of SYNTHESIS OF YNAMIDES BY N-ALKYNYLATION OF AMINE DERIVATIVES. PREPARATION OF N-ALLYL-N-(METHOXYCARBONYL)-1,3-DECADIYNYLAMINE. Submitted by Amanda L. Kohnen, Joshua R. Dunetz, and Rick L… Organic Syntheses
SYNTHESIS OF α,β-UNSATURATED NITRILES FROM ACETONITRILE: CYCLOHEXYLIDENEACETONITRILE AND CINNAMONITRILE (Acetonitrile, cyclohexylidene- and 2-propenenitrile, 3-phenyl, (E)- and (Z)-) Preparation of Acetonitrile, cyclohexylidene- and 2-propenenitrile, 3-phenyl, (E)- and (Z)-. Submitted by Stephen A. DiBiase, James R. Beadle, and George W. Gokel1. DOI: 10.15227/orgsyn.062.0179. Organic Syntheses
SYNTHESIS OF β-KETO ESTERS BY C-ACYLATION OF PREFORMED ENOLATES WITH METHYL CYANOFORMATE: PREPARATION OF METHYL (1α,4aβ,8aα)-2-OXODECAHYDRO-1-NAPHTHOATE Preparation of SYNTHESIS OF β-KETO ESTERS BY C-ACYLATION OF PREFORMED ENOLATES WITH METHYL CYANOFORMATE: PREPARATION OF METHYL (1α,4aβ,8aα)-2-OXODECAHYDRO-1-NAPHTHOATE. Submitted by Simon R. Crabtree,… Organic Syntheses
SYNTHESIS OF β-LACTONES AND ALKENES VIA THIOL ESTERS: (E)-2,3-DIMETHYL-3-DODECENE Preparation of SYNTHESIS OF β-LACTONES AND ALKENES VIA THIOL ESTERS: (E)-2,3-DIMETHYL-3-DODECENE. Submitted by Rick L. Danheiser, James S. Nowick, Janette H. Lee, Raymond F. Miller, and Alexandre H. H… Organic Syntheses
SYNTHESIS OF β-LACTONES BY ALDOLIZATION OF KETONES WITH PHENYL ESTER ENOLATES: 3,3-DIMETHYL-1-OXASPIRO[3.5]NONAN-2-ONE (1-Oxaspiro[3.5]nonan-2-one, 3,3-dimethyl-) Condensation Preparation of 1-Oxaspiro[3.5]nonan-2-one, 3,3-dimethyl-. Submitted by Christine Wedler and Hans Schick1. DOI: 10.15227/orgsyn.075.0116. Organic Syntheses
SYRINGIC ALDEHYDE (Syringaldehyde) Preparation of Syringaldehyde. Submitted by C. F. H. Allen and Gerhard W. Leubner1. DOI: 10.15227/orgsyn.031.0092. Organic Syntheses
(S)-(−)-α-(1-NAPHTHYL)ETHYLAMINE ((S)-1-Naphthalenemethanamine, α-methyl-) Preparation of (S)-1-Naphthalenemethanamine, α-methyl-. Submitted by E. Mohacsi and W. Leimgruber1. DOI: 10.15227/orgsyn.055.0080. Organic Syntheses
(S)-(+)-γ-BUTYROLACTONE-γ-CARBOXYLIC ACID (2-Furancarboxylic acid, tetrahydro-5-oxo-, (S)-) Preparation of 2-Furancarboxylic acid, tetrahydro-5-oxo-, (S)-. Submitted by Olivier H. Gringore and Francis P. Rouessac1. DOI: 10.15227/orgsyn.063.0121. Organic Syntheses
TANDEM NUCLEOPHILIC ADDITION / FRAGMENTATION OF VINYLOGOUS ACYL TRIFLATES: 2-METHYL-2-(1-OXO-5-HEPTYNYL)-1,3-DITHIANE Addition Preparation of TANDEM NUCLEOPHILIC ADDITION / FRAGMENTATION OF VINYLOGOUS ACYL TRIFLATES: 2-METHYL-2-(1-OXO-5-HEPTYNYL)-1,3-DITHIANE. Submitted by Marilda P. Lisboa, Tung T. Hoang, and Gregory B. Dudl… Organic Syntheses
TAURINE (I) Preparation of I. Submitted by C. S. Marvel and C. F. Bailey. DOI: 10.15227/orgsyn.018.0077. Organic Syntheses
t-BUTYL ACETOACETATE (Acetoacetic acid, tert-butyl ester) Preparation of Acetoacetic acid, tert-butyl ester. Submitted by Sven-Olov Lawesson, Susanne Gronwall, and Rune Sandberg1. DOI: 10.15227/orgsyn.042.0028. Organic Syntheses
t-Butyl as a Pyrazole Protecting Group: Preparation and Use of 1-tert-Butyl-3-Methyl-1H-Pyrazole-5-Amine Preparation of t-Butyl as a Pyrazole Protecting Group: Preparation and Use of 1-tert-Butyl-3-Methyl-1H-Pyrazole-5-Amine. Submitted by Patrick M. Pollock and Kevin P. Cole1. DOI: 10.15227/orgsyn.089.05… Organic Syntheses
t-BUTYL AZIDOFORMATE (Formic acid, azido-, tert-butyl ester) Preparation of Formic acid, azido-, tert-butyl ester. Submitted by Louis A. Carpino, Barbara A. Carpino, Paul J. Crowley, Chester A. Giza, and Paul H. Terry1. DOI: 10.15227/orgsyn.044.0015. Organic Syntheses
t-BUTYL AZODIFORMATE (Formic acid, azodi-, di-tert-butyl ester) Preparation of Formic acid, azodi-, di-tert-butyl ester. Submitted by Louis A. Carpino and Paul J. Crowley1. DOI: 10.15227/orgsyn.044.0018. Organic Syntheses
t-BUTYL CARBAMATE (Carbamic acid, tert-butyl ester) Preparation of Carbamic acid, tert-butyl ester. Submitted by Bernard Loev, Minerva F. Kormendy, and Marjorie M. Goodman1. DOI: 10.15227/orgsyn.048.0032. Organic Syntheses
t-BUTYL CARBAZATE (Carbazic acid, tert-butyl ester) Preparation of Carbazic acid, tert-butyl ester. Submitted by Louis A. Carpino, David Collins, Siegfried Göwecke, Joe Mayo, S. D. Thatte, and Fred Tibbetts1. DOI: 10.15227/orgsyn.044.0020. Organic Syntheses
t-BUTYL CYANOACETATE (Cyanoacetic acid, tert-butyl ester) Preparation of Cyanoacetic acid, tert-butyl ester. Submitted by Robert E. Ireland and Michael Chaykovsky1. DOI: 10.15227/orgsyn.041.0005. Organic Syntheses
t-BUTYL DIAZOACETATE (Acetic acid, diazo-, tert-butyl ester) Preparation of Acetic acid, diazo-, tert-butyl ester. Submitted by Manfred Regitz, Jürgen Hocker, and Annemarie Liedhegener1. DOI: 10.15227/orgsyn.048.0036. Organic Syntheses
t-BUTYL HYPOCHLORITE Preparation of t-BUTYL HYPOCHLORITE. Submitted by M. J. Mintz1 and C. Walling2. DOI: 10.15227/orgsyn.049.0009. Organic Syntheses
TELOMERIZATION OF ISOPRENE WITH DIALKYLAMINE: N,N-DIETHYLNERYLAMINE (2,6-Octadien-1-amine, N,N-diethyl-3,7-dimethyl-, (Z)-) Preparation of 2,6-Octadien-1-amine, N,N-diethyl-3,7-dimethyl-, (Z)-. Submitted by Kunihiko Takabe1, Takashi Yamada, Takao Katagiri1, and Juntaro Tanaka1. DOI: 10.15227/orgsyn.067.0048. Organic Syntheses
TEREPHTHALALDEHYDE Preparation of TEREPHTHALALDEHYDE. Submitted by J. M. Snell and A. Weissberger. DOI: 10.15227/orgsyn.020.0092. Organic Syntheses
TEREPHTHALIC ACID Preparation of TEREPHTHALIC ACID. Submitted by C. F. Koelsch. DOI: 10.15227/orgsyn.026.0095. Organic Syntheses
tert-BUTOXYCARBONYLATION OF AMINO ACIDS AND THEIR DERIVATIVES: N-tert-BUTOXYCARBONYL-l-PHENYLALANINE (L-Phenylalanine, N-[(1,1-dimethylethoxy)carbonyl]-) Preparation of L-Phenylalanine, N-[(1,1-dimethylethoxy)carbonyl]-. Submitted by Oskar Keller, Walter E. Keller, Gert van Look, and Gernot Wersin1. DOI: 10.15227/orgsyn.063.0160. Organic Syntheses
tert-BUTOXYCARBONYL-L-PROLINE (1,2-Pyrrolidinedicarboxylic acid, 1-(1,1-dimethylethyl) ester, (S)-) Preparation of 1,2-Pyrrolidinedicarboxylic acid, 1-(1,1-dimethylethyl) ester, (S)-. Submitted by Ulf Ragnarsson1, Sune M. Karlsson, Bengt E. Sandberg, and Lars-Eric Larsson. DOI: 10.15227/orgsyn.053.0… Organic Syntheses
tert-BUTYL ACETATE (Acetic acid, tert-butyl ester) Preparation of Acetic acid, tert-butyl ester. Submitted by Robert H. Baker and Frederick G. Bordwell. DOI: 10.15227/orgsyn.024.0018. Organic Syntheses
tert-BUTYL ACETOTHIOACETATE AND ITS USE IN SYNTHESIS: 3-ACETYL-4-HYDROXY-5,5-DIMETHYLFURAN-2(4H)-ONE (Acetoacetic acid, 1-thio-, S-tert-butyl ester) Preparation of Acetoacetic acid, 1-thio-, S-tert-butyl ester. Submitted by Christina M. J. Fox and Steven V. Ley1. DOI: 10.15227/orgsyn.066.0108. Organic Syntheses
tert-BUTYLAMINE (I. HYDROGENOLYSIS OF 2,2-DIMETHYLETHYLENIMINE) Preparation of I. HYDROGENOLYSIS OF 2,2-DIMETHYLETHYLENIMINE. Submitted by Kenneth N. Campbell, Armiger H. Sommers, and Barbara K. Campbell. DOI: 10.15227/orgsyn.029.0018. Organic Syntheses
tert-BUTYL AZIDOFORMATE (Carbonazidic acid, 1,1-dimethylethyl ester) Preparation of Carbonazidic acid, 1,1-dimethylethyl ester. Submitted by Michael A. Insalaco and D. Stanley Tarbell1. DOI: 10.15227/orgsyn.050.0009. Organic Syntheses
tert.-BUTYL CHLORIDE (Propane, 2-chloro-2-methyl-) Preparation of Propane, 2-chloro-2-methyl-. Submitted by James F. Norris and Alanson W. Olmsted. DOI: 10.15227/orgsyn.008.0050. Organic Syntheses
tert-BUTYLCYANOKETENE (Butanenitrile, 2-carbonyl-3,3-dimethyl-) Preparation of Butanenitrile, 2-carbonyl-3,3-dimethyl-. Submitted by Walter Weyler, Jr., Warren G. Duncan, Margo Beth Liewen, and Harold W. Moore1. DOI: 10.15227/orgsyn.055.0032. Organic Syntheses
(tert-BUTYLDIMETHYLSILYL)ALLENE (Silane, (1,1-dimethylethyl)dimethyl-1,2-propadienyl-) Preparation of Silane, (1,1-dimethylethyl)dimethyl-1,2-propadienyl-. Submitted by Andrew G. Myers and Bin Zheng1. DOI: 10.15227/orgsyn.076.0178. Organic Syntheses
tert-BUTYL HYPOCHLORITE Preparation of tert-BUTYL HYPOCHLORITE. Submitted by H. M. Teeter and E. W. Bell1. DOI: 10.15227/orgsyn.032.0020. Organic Syntheses
TERT-BUTYL TERT-BUTYLDIMETHYLSILYLGLYOXYLATE: A USEFUL CONJUNCTIVE REAGENT Preparation of TERT-BUTYL TERT-BUTYLDIMETHYLSILYLGLYOXYLATE: A USEFUL CONJUNCTIVE REAGENT. Submitted by David A. Nicewicz, Guillaume Brétéché, and Jeffrey S. Johnson1. DOI: 10.15227/orgsyn.085.0278. Organic Syntheses
tert-BUTYL-tert-OCTYLAMINE (2-Pentanamine, N-(1,1-dimethylethyl)-2,4,4-trimethyl-) Preparation of 2-Pentanamine, N-(1,1-dimethylethyl)-2,4,4-trimethyl-. Submitted by E. J. Corey and Andrew W. Gross1. DOI: 10.15227/orgsyn.065.0166. Organic Syntheses
TERTIARY ALCOHOLS FROM HYDROCARBONS BY OZONATION ON SILICA GEL: 1-ADAMANTANOL (Tricyclo[3.3.1.13,7]decan-1-ol) Preparation of Tricyclo[3.3.1.13,7]decan-1-ol. Submitted by Zvi Cohen, Haim Varkony, Ehud Keinan, and Yehuda Mazur1. DOI: 10.15227/orgsyn.059.0176. Organic Syntheses
TETRAACETYLETHANE (2,5-Hexanedione, 3,4-diacetyl-) Preparation of 2,5-Hexanedione, 3,4-diacetyl-. Submitted by Robert G. Charles1. DOI: 10.15227/orgsyn.039.0061. Organic Syntheses
TETRABENZYL PYROPHOSPHATE ([Diphosphoric acid, tetrakis(phenylmethyl) ester]) Preparation of [Diphosphoric acid, tetrakis(phenylmethyl) ester]. Submitted by Todd D. Nelson1, Jonathan D. Rosen1, M. Bhupathy1, James McNamara1, Michael J. Sowa2, Chad Rush2, and Louis S. Crocker3. … Organic Syntheses
TETRACYANOETHYLENE (Ethenetetracarbonitrile) Preparation of Ethenetetracarbonitrile. Submitted by R. A. Carboni1. DOI: 10.15227/orgsyn.039.0064. Organic Syntheses
TETRACYANOETHYLENE OXIDE (Ethanetetracarbonitrile, 1,2-epoxy-) Preparation of Ethanetetracarbonitrile, 1,2-epoxy-. Submitted by W. J. Linn1. DOI: 10.15227/orgsyn.049.0103. Organic Syntheses
TETRAETHYLTIN (Tin, tetraethyl-) Preparation of Tin, tetraethyl-. Submitted by G. J. M. Van Der Kerk and J. G. A. Luijten1. DOI: 10.15227/orgsyn.036.0086. Organic Syntheses

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