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2861 reactions imported from Wikipedia named-reactions and Organic Syntheses archives. Filter by source or search by name + summary.

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Equation Name Summary Source
Preparation of Cyclobutenone Preparation of Preparation of Cyclobutenone. Submitted by Audrey G. Ross, Xiaohua Li, and Samuel J. Danishefsky1. DOI: 10.15227/orgsyn.089.0491. Organic Syntheses
PREPARATION OF CYCLOHEPTANE-1,3-DIONE VIA REDUCTIVE RING EXPANSION OF 1-TRIMETHYLSILYLOXY-7,7-DICHLOROBICYCLO[3.2.0]HEPTAN-6-ONE (Cycloheptane-1,3-dione) Preparation of Cycloheptane-1,3-dione. Submitted by Nga Do, Ruth E. McDermott, and John A. Ragan1a. DOI: 10.15227/orgsyn.085.0138. Organic Syntheses
Preparation of DABSO from Karl-Fischer reagent Preparation of Preparation of DABSO from Karl-Fischer reagent. Submitted by Ludovic Martial and Laurent Bischoff. *1. DOI: 10.15227/orgsyn.090.0301. Organic Syntheses
PREPARATION OF (E)-1-DIMETHYLAMINO-3-tert-BUTYLDIMETHYLSILOXY-1,3-BUTADIENE (1,3-Butadien-1-amine, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N,N-dimethyl-) Preparation of 1,3-Butadien-1-amine, 3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-N,N-dimethyl-. Submitted by Sergey A. Kozmin, Shuwen He, and Viresh H. Rawal1. DOI: 10.15227/orgsyn.078.0152. Organic Syntheses
PREPARATION OF (E)-(2-IODOVINYL)BENZENE FROM BENZYL BROMIDE AND DIIODOMETHANE ((E)-β-STYRYL IODIDE) Preparation of (E)-β-STYRYL IODIDE. Submitted by James A. Bull, James J. Mousseau, and André B. Charette1. DOI: 10.15227/orgsyn.087.0170. Organic Syntheses
Preparation of Enantioenriched Homoallylic Primary Amines Preparation of Preparation of Enantioenriched Homoallylic Primary Amines. Submitted by José C. González-Gómez, Francisco Foubelo, and Miguel Yus1. DOI: 10.15227/orgsyn.089.0088. Organic Syntheses
PREPARATION OF ENANTIOMERICALLY ENRICHED (1S)-1-PHENYLPROPAN-1-AMINE HYDROCHLORIDE BY A CATALYTIC ADDITION OF DIORGANOZINC REAGENTS TO IMINES (Benzenemethanamine, α-ethyl-, hydrochloride, (αS)-) Addition Preparation of Benzenemethanamine, α-ethyl-, hydrochloride, (αS)-. Submitted by Jean-Nicolas Desrosiers, Alexandre Côté, Alessandro A. Boezio, and André B. Charette1. DOI: 10.15227/orgsyn.083.0005. Organic Syntheses
PREPARATION OF ENANTIOMERICALLY PURE (R,R)-BozPHOS ((2R,5R)-1-{2-[(2R,5R)-2,5-dimethylphospholan-1-yl]phenyl}-2,5-dimethylphospholane 1-oxide) Preparation of (2R,5R)-1-{2-[(2R,5R)-2,5-dimethylphospholan-1-yl]phenyl}-2,5-dimethylphospholane 1-oxide. Submitted by Alexandre Côté, Jean-Nicolas Desrosiers, Alessandro A. Boezio, and André B. Chare… Organic Syntheses
PREPARATION OF ENANTIOMERICALLY PURE α-N,N-DIBENZYLAMINO ALDEHYDES: S-2-(N,N-DIBENZYLAMINO)-3-PHENYLPROPANAL (Benzenepropanal, α-[bis(phenylmethyl)amino]-, (S)-) Preparation of Benzenepropanal, α-[bis(phenylmethyl)amino]-, (S)-. Submitted by Manfred T. Reetz1 , Mark W. Drewes2 , and Renate Schwickardi1. DOI: 10.15227/orgsyn.076.0110. Organic Syntheses
Preparation of (E)-N,N-Diethyl-2-styrylbenzamide by Rh-Catalyzed C-H Activation Preparation of Preparation of (E)-N,N-Diethyl-2-styrylbenzamide by Rh-Catalyzed C-H Activation. Submitted by Frederic W. Patureau, Tatiana Besset, and Frank Glorius1. DOI: 10.15227/orgsyn.090.0041. Organic Syntheses
PREPARATION OF ETHYL 1-BENZYL-4-FLUOROPIPERIDINE-4-CARBOXYLATE Preparation of PREPARATION OF ETHYL 1-BENZYL-4-FLUOROPIPERIDINE-4-CARBOXYLATE. Submitted by Jianshe Kong1*, Tao Meng1, Pauline Ting1, and Jesse Wong1. DOI: 10.15227/orgsyn.087.0137. Organic Syntheses
Preparation of H,4 PyrrolidineQuin-BAM (PBAM) Preparation of Preparation of H,4 PyrrolidineQuin-BAM (PBAM). Submitted by Tyler A. Davis, Mark C. Dobish, Kenneth E. Schwieter, Aspen C. Chun, and Jeffrey N. Johnston1. DOI: 10.15227/orgsyn.089.0380. Organic Syntheses
PREPARATION OF HEXAKIS(4-BROMOPHENYL)BENZENE (HBB) (1,1':2',1"-Terphenyl, 4,4"-dibromo-3',4',5',6'-tetrakis(4-bromophenyl)-) Preparation of 1,1':2',1"-Terphenyl, 4,4"-dibromo-3',4',5',6'-tetrakis(4-bromophenyl)-. Submitted by Rajendra Rathore1 and Carrie L. Burns. DOI: 10.15227/orgsyn.082.0030. Organic Syntheses
PREPARATION OF HORNER-WADSWORTH-EMMONS REAGENT: METHYL 2-BENZYLOXYCARBONYLAMINO-2- (DIMETHOXY- PHOSPHINYL)ACETATE Olefination Preparation of PREPARATION OF HORNER-WADSWORTH-EMMONS REAGENT: METHYL 2-BENZYLOXYCARBONYLAMINO-2- (DIMETHOXY- PHOSPHINYL)ACETATE. Submitted by Hiroki Azuma1, Kentaro Okano1, Tohru Fukuyama2, and Hidet… Organic Syntheses
PREPARATION OF HYDRAZONES: ACETOPHENONE HYDRAZONE (Ethanone, 1-phenyl-, hydrazone) Preparation of Ethanone, 1-phenyl-, hydrazone. Submitted by G. R. Newkome1 and D. L. Fishel2. DOI: 10.15227/orgsyn.050.0102. Organic Syntheses
PREPARATION OF ISOPROPYL 2-DIAZOACETYL(PHENYL)CARBAMATE Preparation of PREPARATION OF ISOPROPYL 2-DIAZOACETYL(PHENYL)CARBAMATE. Submitted by Hubert Muchalski, Amanda B. Doody, Timothy L. Troyer, and Jeffrey N. Johnston1. DOI: 10.15227/orgsyn.088.0212. Organic Syntheses
PREPARATION OF LOW-HALIDE METHYLLITHIUM (Lithium, methyl-) Preparation of Lithium, methyl-. Submitted by Michael J. Lusch, William V. Phillips, Ronald F. Sieloff, Glenn S. Nomura, and Herbert O. House1. DOI: 10.15227/orgsyn.062.0101. Organic Syntheses
Preparation of N1-Phenylacetamidine 4-Bromobenzoate Using 2,2,2-Trichloroethyl Acetimidate Hydrochloride Preparation of Preparation of N1-Phenylacetamidine 4-Bromobenzoate Using 2,2,2-Trichloroethyl Acetimidate Hydrochloride. Submitted by Lulin Wei and Stéphane Caron1. DOI: 10.15227/orgsyn.090.0174. Organic Syntheses
PREPARATION OF N-AMINOAZIRIDINES: trans-1-AMINO-2,3-DIPHENYLAZIRIDINE, 1-AMINO-2-PHENYLAZIRIDINE, AND 1-AMINO-2-PHENYLAZIRIDINIUM ACETATE (1-Aziridinamine, trans-(±)-2,3-diphenyl-, 1-aziridinamine, (±)-2-phenyl-, and 1-aziridinamine, monoacetate, (±)-2-phenyl-) Preparation of 1-Aziridinamine, trans-(±)-2,3-diphenyl-, 1-aziridinamine, (±)-2-phenyl-, and 1-aziridinamine, monoacetate, (±)-2-phenyl-. Submitted by Robert K. Müller, Renato Joos, Dorothee Felix, Ja… Organic Syntheses
PREPARATION OF N-ARYL-5R-HYDROXYMETHYL-2-OXAZOLIDINONES FROM N-ARYL CARBAMATES: N-PHENYL-(5R)-HYDROXYMETHYL- 2-OXAZOLIDINONE (2-Oxazolidinone, 5-(hydroxymethyl)-3-phenyl-, (5R)-) Preparation of 2-Oxazolidinone, 5-(hydroxymethyl)-3-phenyl-, (5R)-. Submitted by Peter R. Manninen1 and Steven J. Brickner.2. DOI: 10.15227/orgsyn.081.0112. Organic Syntheses
PREPARATION OF n-BUTYL 4-CHLOROPHENYL SULFIDE Preparation of PREPARATION OF n-BUTYL 4-CHLOROPHENYL SULFIDE. Submitted by J. Christopher McWilliams1 , Fred J. Fleitz, Nan Zheng, and Joseph D. Armstrong III. DOI: 10.15227/orgsyn.079.0043. Organic Syntheses
Preparation of n-Isopropylidene-n'-2-Nitrobenzenesulfonyl Hydrazine (IPNBSH) and Its Use in Palladium-catalyzed Synthesis of Monoalkyl Diazenes. Synthesis of 9-Allylanthracene Preparation of Preparation of n-Isopropylidene-n'-2-Nitrobenzenesulfonyl Hydrazine (IPNBSH) and Its Use in Palladium-catalyzed Synthesis of Monoalkyl Diazenes. Synthesis of 9-Allylanthracene. Submitte… Organic Syntheses
PREPARATION OF N-p-TOLYLSULFONYL-(E)-1-PHENYLETHYLIDENEIMINE Preparation of PREPARATION OF N-p-TOLYLSULFONYL-(E)-1-PHENYLETHYLIDENEIMINE. Submitted by José Luis García Ruano, José Alemán, Alejandro Parra, and M. Belén Cid1. DOI: 10.15227/orgsyn.084.0129. Organic Syntheses
PREPARATION OF O-ALLYL-N-(9-ANTHRACENYLMETHYL)CINCHONIDINIUM BROMIDE AS A PHASE TRANSFER CATALYST FOR THE ENANTIOSELECTIVE ALKYLATION OF GLYCINE BENZOPHENONE IMINE tert-BUTYL ESTER: (4S)-2-(BENZHYDRYLIDENAMINO)PENTANEDIOIC ACID, 1-tert-BUTYL ESTER-5-METHYL ESTER ([Cinchonanium, 1-(9-anthracenylmethyl)-9-(2-propenyloxy)-, bromide, (8α,9R)-and L-Glutamic acid, N-(diphenylmethylene)-, 1-(1,1-dimethylethyl) 5-methyl ester]) Preparation of [Cinchonanium, 1-(9-anthracenylmethyl)-9-(2-propenyloxy)-, bromide, (8α,9R)-and L-Glutamic acid, N-(diphenylmethylene)-, 1-(1,1-dimethylethyl) 5-methyl ester]. Submitted by E. J. Corey1… Organic Syntheses
PREPARATION OF O-ESTERS FROM THE CORRESPONDING THIOL ESTERS: tert-BUTYL CYCLOHEXANECARBOXYLATE (Cyclohexanecarboxylic acid, 1,1-dimethylethyl ester) Preparation of Cyclohexanecarboxylic acid, 1,1-dimethylethyl ester. Submitted by Wan Kit Chan1, S. Masamune1, and Gary O. Spessard2. DOI: 10.15227/orgsyn.061.0048. Organic Syntheses
PREPARATION OF OPTICALLY ACTIVE (R,R)-HYDROBENZOIN FROM BENZOIN OR BENZIL (1,2-Ethanediol, 1,2-diphenyl-, (1R,2R)-) Preparation of 1,2-Ethanediol, 1,2-diphenyl-, (1R,2R)-. Submitted by Takao Ikariya1, Shohei Hashiguchi2, Kunihiko Murata3, and Ryoji Noyori4. DOI: 10.15227/orgsyn.082.0010. Organic Syntheses
PREPARATION OF PIVALOYL HYDRAZIDE IN WATER (Propanoic acid, 2,2-dimethyl-, hydrazide) Preparation of Propanoic acid, 2,2-dimethyl-, hydrazide. Submitted by Bryan Li, 1, Raymond J. Bemish, David R. Bill, Steven Brenek, Richard A. Buzon, Charles K-F Chiu, and Lisa Newell. DOI: 10.15227/o… Organic Syntheses
PREPARATION OF POLYQUINANES BY DOUBLE ADDITION OF VINYL ANIONS TO SQUARATE ESTERS: 4,5,6,6a-TETRAHYDRO-3a-HYDROXY-2,3-DIISOPROPOXY-4,6a-DIMETHYL-1(3aH)-PENTALENONE Addition Preparation of PREPARATION OF POLYQUINANES BY DOUBLE ADDITION OF VINYL ANIONS TO SQUARATE ESTERS: 4,5,6,6a-TETRAHYDRO-3a-HYDROXY-2,3-DIISOPROPOXY-4,6a-DIMETHYL-1(3aH)-PENTALENONE. Submitted by Tina Mo… Organic Syntheses
Preparation of (R)-4-Cyclohexyl-2,3-butadien-1-ol Preparation of Preparation of (R)-4-Cyclohexyl-2,3-butadien-1-ol. Submitted by Juntao Ye and Shengming Ma*1. DOI: 10.15227/orgsyn.091.0233. Organic Syntheses
Preparation of (Ra)-Methyl 3-(dimethyl(phenyl)silyl)hexa-3,4-dienoate Preparation of Preparation of (Ra)-Methyl 3-(dimethyl(phenyl)silyl)hexa-3,4-dienoate. Submitted by Ryan A. Brawn and James S. Panek1. DOI: 10.15227/orgsyn.089.0420. Organic Syntheses
PREPARATION OF (R,R)-1,2:4,5-DIEPOXYPENTANE (D-threo-Pentitol, 1,2:4,5-dianhydro-3-deoxy-) Preparation of D-threo-Pentitol, 1,2:4,5-dianhydro-3-deoxy-. Submitted by Scott D. Rychnovsky, George Griesgraber, and Jay P. Powers1. DOI: 10.15227/orgsyn.077.0001. Organic Syntheses
PREPARATION OF [R-(R,S)]-β-METHYL-α-PHENYL-1-PYRROLIDINEETHANOL (1-Pyrrolidineethanol, β-methyl-α-phenyl-, [R-(R,S)]-) Preparation of 1-Pyrrolidineethanol, β-methyl-α-phenyl-, [R-(R,S)]-. Submitted by Dalian Zhao, Cheng-yi Chen, Feng Xu, Lushi Tan, Richard Tillyer1 , Michael E. Pierce, and James R. Moore2. DOI: 10.152… Organic Syntheses
PREPARATION OF (S)-2-ALLYL-2-METHYLCYCLOHEXANONE (Cyclohexanone, 2-methyl-2-(2-propen-1-yl)-, (2S)-) Preparation of Cyclohexanone, 2-methyl-2-(2-propen-1-yl)-, (2S)-. Submitted by Justin T. Mohr, Michael R. Krout, and Brian M. Stoltz.*1. DOI: 10.15227/orgsyn.086.0194. Organic Syntheses
PREPARATION OF (S)-3,3'-BIS-MORPHOLINOMETHYL-5,5',6,6',7,7',8,8'-OCTAHYDRO-1,1'-BI-2-NAPHTHOL Preparation of PREPARATION OF (S)-3,3'-BIS-MORPHOLINOMETHYL-5,5',6,6',7,7',8,8'-OCTAHYDRO-1,1'-BI-2-NAPHTHOL. Submitted by Mark Turlington and Lin Pu1. DOI: 10.15227/orgsyn.087.0059. Organic Syntheses
PREPARATION OF (S)-4-ISOPROPYL-N-PROPANOYL-1,3-THIAZOLIDINE-2-THIONE Preparation of PREPARATION OF (S)-4-ISOPROPYL-N-PROPANOYL-1,3-THIAZOLIDINE-2-THIONE. Submitted by Erik Gálvez, Pedro Romea, and Fèlix Urpí1. DOI: 10.15227/orgsyn.086.0070. Organic Syntheses
PREPARATION OF SECONDARY AMINES FROM PRIMARY AMINES VIA 2-NITROBENZENESULFONAMIDES: N-(4-METHOXYBENZYL)-3-PHENYLPROPYLAMINE (Benzenepropanamine, N-[(4-methoxyphenyl)methyl]-) Preparation of Benzenepropanamine, N-[(4-methoxyphenyl)methyl]-. Submitted by Wataru Kurosawa, Toshiyuki Kan, and Tohru Fukuyama1. DOI: 10.15227/orgsyn.079.0186. Organic Syntheses
PREPARATION OF (S)-METHYL GLYCIDATE VIA HYDROLYTIC KINETIC RESOLUTION (Oxiranecarboxylic Acid, Methyl Ester, (2S)-) Preparation of Oxiranecarboxylic Acid, Methyl Ester, (2S)-. Submitted by Christian P. Stevenson, Lars P. C. Nielsen, and Eric N. Jacobsen1. DOI: 10.15227/orgsyn.083.0162. Organic Syntheses
PREPARATION OF (S,S)-1,2-BIS(tert-BUTYLMETHYLPHOSPHINO)ETHANE ((S,S)-t-Bu-BISP*) AS A RHODIUM COMPLEX (Rhodium(1+), [(2,3,5,6-η)-bicyclo[2.2.1]hepta-2,5-diene](S,S)-1,2-bis(tert-butylmethylphosphino)ethane, tetrafluoroborate(1−)) Preparation of Rhodium(1+), [(2,3,5,6-η)-bicyclo[2.2.1]hepta-2,5-diene](S,S)-1,2-bis(tert-butylmethylphosphino)ethane, tetrafluoroborate(1−). Submitted by Karen V. L. Crépy and Tsuneo Imamoto1. DOI: 1… Organic Syntheses
PREPARATION OF (S)-tert-ButylPHOX (Oxazole, 4-(1,1-dimethylethyl)-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro- (4S)-) Preparation of Oxazole, 4-(1,1-dimethylethyl)-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro- (4S)-. Submitted by Michael R. Krout, Justin T. Mohr, and Brian M. Stoltz.*1. DOI: 10.15227/orgsyn.086.0181. Organic Syntheses
PREPARATION OF SUBSTITUTED 5-AZAINDOLES: METHYL 4-CHLORO-1H-PYRROLO[3,2-C]PYRIDINE-2-CARBOXYLATE Preparation of PREPARATION OF SUBSTITUTED 5-AZAINDOLES: METHYL 4-CHLORO-1H-PYRROLO[3,2-C]PYRIDINE-2-CARBOXYLATE. Submitted by Patrick Roy1, Michel Boisvert, and Yves Leblanc. DOI: 10.15227/orgsyn.084.… Organic Syntheses
PREPARATION OF SUBSTITUTED PYRIDINES VIA REGIOCONTROLLED [4 + 2] CYCLOADDITIONS OF OXIMINOSULFONATES: METHYL 5-METHYLPYRIDINE-2-CARBOXYLATE ((2-Pyridinecarboxylic acid, 5-methyl-, methyl ester)) Cycloaddition Preparation of (2-Pyridinecarboxylic acid, 5-methyl-, methyl ester). Submitted by Rick L. Danheiser, Adam R. Renslo, David T. Amos, and Graham T. Wright.1. DOI: 10.15227/orgsyn.080.0133. Organic Syntheses
Preparation of t-Butyl-3-Bromo-5-Formylbenzoate Through Selective Metal-Halogen Exchange Reactions Preparation of Preparation of t-Butyl-3-Bromo-5-Formylbenzoate Through Selective Metal-Halogen Exchange Reactions. Submitted by Juan D. Arredondo, Hongmei Li, and Jaume Balsells1. DOI: 10.15227/orgsyn… Organic Syntheses
Preparation of Tetrabutylammonium(4-Fluorophenyl)trifluoroborate Preparation of Preparation of Tetrabutylammonium(4-Fluorophenyl)trifluoroborate. Submitted by Fabrizio Pertusati, Parag V. Jog, and G. K. Surya Prakash. *1. DOI: 10.15227/orgsyn.090.0261. Organic Syntheses
Preparation of Tetrahydroisoquinoline-3-ones Via Cyclization of Phenyl Acetamides Using Eaton's Reagent Cyclization Preparation of Preparation of Tetrahydroisoquinoline-3-ones Via Cyclization of Phenyl Acetamides Using Eaton's Reagent. Submitted by Qiang Yang, Luckner G. Ulysse, Mark D. McLaws, Daniel K. Keefe, Pet… Organic Syntheses
PREPARATION OF THE COP CATALYSTS: [(S)-COP-OAc]2, [(S)-COP-Cl]2, AND (S)-COP-hfacac Preparation of PREPARATION OF THE COP CATALYSTS: [(S)-COP-OAc]2, [(S)-COP-Cl]2, AND (S)-COP-hfacac. Submitted by Carolyn E. Anderson, Stefan F. Kirsch, Larry E. Overman*1, Christopher J. Richards, and… Organic Syntheses
PREPARATION OF THIOL ESTERS: S-tert-BUTYL CYCLOHEXANECARBOTHIOATE AND S-tert-BUTYL 3α,7α,12α-TRIHYDROXY-5β-CHOLANE-24-THIOATE (Cyclohexanecarbothioic acid, S-(1,1-dimethylethyl)ester and cholane-24-thioic acid, 3,7,12-trihydroxy-S-(1,1-dimethylethyl)ester, (3α,5β,7α,12α)) Preparation of Cyclohexanecarbothioic acid, S-(1,1-dimethylethyl)ester and cholane-24-thioic acid, 3,7,12-trihydroxy-S-(1,1-dimethylethyl)ester, (3α,5β,7α,12α). Submitted by Gary O. Spessard1, Wan Kit… Organic Syntheses
PREPARATION OF (TRIPHENYLPHOSPHORANYLIDENE)-KETENE FROM (METHOXYCARBONYLMETHYLENE)-TRIPHENYLPHOSPHORANE Preparation of PREPARATION OF (TRIPHENYLPHOSPHORANYLIDENE)-KETENE FROM (METHOXYCARBONYLMETHYLENE)-TRIPHENYLPHOSPHORANE. Submitted by Rainer Schobert1. DOI: 10.15227/orgsyn.082.0140. Organic Syntheses
PREPARATION OF VINYL TRIFLUOROMETHANESULFONATES: 3-METHYL-2-BUTEN-2-YL TRIFLATE (Methanesulfonic acid, trifluoro-, 1,2-dimethyl-1-propenyl ester) Preparation of Methanesulfonic acid, trifluoro-, 1,2-dimethyl-1-propenyl ester. Submitted by Peter J. Stang1 and Thomas E. Dueber. DOI: 10.15227/orgsyn.054.0079. Organic Syntheses
PREPARATION OF α-ACETOXY ETHERS BY THE REDUCTIVE ACETYLATION OF ESTERS: endo-1-BORNYLOXYETHYL ACETATE ((Ethanol, 1-[[(1R,2S,4R)-1,7,7-trimethylbicyclo[2.2.1]hept-2-yl]oxy]-, acetate)) Preparation of (Ethanol, 1-[[(1R,2S,4R)-1,7,7-trimethylbicyclo[2.2.1]hept-2-yl]oxy]-, acetate). Submitted by David J. Kopecky and Scott D. Rychnovsky1. DOI: 10.15227/orgsyn.080.0177. Organic Syntheses
Preparation of α-Fluorobis(phenylsulfonyl)methane (FBSM) Preparation of Preparation of α-Fluorobis(phenylsulfonyl)methane (FBSM). Submitted by G. K. Surya Prakash, Nan Shao, Fang Wang, and Chuanfa Ni1. DOI: 10.15227/orgsyn.090.0130. Organic Syntheses

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