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2861 reactions imported from Wikipedia named-reactions and Organic Syntheses archives. Filter by source or search by name + summary.

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Equation Name Summary Source
Practical Synthesis of Di-tert-Butyl-Phosphinoferrocene Preparation of Practical Synthesis of Di-tert-Butyl-Phosphinoferrocene. Submitted by Carl A. Busacca, Magnus C. Eriksson,1 Nizar Haddad, Z. Steve Han, Jon C. Lorenz, Bo Qu, Xingzhong Zeng, and Chris H… Organic Syntheses
PRACTICAL SYNTHESIS OF NOVEL CHIRAL ALLENAMIDES: (R)-4-PHENYL-3-(1,2-PROPADIENYL)OXAZOLIDIN-2-ONE (2-Oxazolidinone, 4-phenyl-3-(1,2-propadienyl)-, (4R)-) Preparation of 2-Oxazolidinone, 4-phenyl-3-(1,2-propadienyl)-, (4R)-. Submitted by H. Xiong, M. R. Tracey, T. Grebe, J. A. Mulder, and R. P. Hsung1. DOI: 10.15227/orgsyn.081.0147. Organic Syntheses
PREPARATION AND [2+2] CYCLOADDITION OF 1-TRIISOPROPYLSILOXY-1-HEXYNE WITH METHYL CROTONATE: 3-BUTYL-4-METHYL-2-TRIISOPROPYLSILOXY-CYCLOBUT-2-ENECARBOXYLIC ACID METHYL ESTER Cycloaddition Preparation of PREPARATION AND [2+2] CYCLOADDITION OF 1-TRIISOPROPYLSILOXY-1-HEXYNE WITH METHYL CROTONATE: 3-BUTYL-4-METHYL-2-TRIISOPROPYLSILOXY-CYCLOBUT-2-ENECARBOXYLIC ACID METHYL ESTER. Submitted b… Organic Syntheses
PREPARATION AND DIELS-ALDER REACTION OF A 2-AMIDO SUBSTITUTED FURAN: tert-BUTYL 3a-METHYL-5-OXO-2,3,3a,4,5,6-HEXAHYDROINDOLE-1-CARBOXYLATE (1H-Indole-1-carboxylic acid, 2,3,3a,4,5,6-hexahydro-3a-methyl-5-oxo-, 1,1-dimethylethyl ester) Preparation of 1H-Indole-1-carboxylic acid, 2,3,3a,4,5,6-hexahydro-3a-methyl-5-oxo-, 1,1-dimethylethyl ester. Submitted by Albert Padwa1 , Michael A. Brodney, and Stephen M. Lynch. DOI: 10.15227/orgsy… Organic Syntheses
PREPARATION AND DIELS–ALDER REACTION OF A HIGHLY NUCLEOPHILIC DIENE: trans-1-METHOXY-3-TRIMETHYLSILOXY-1,3-BUTADIENE AND 5β-METHOXYCYCLOHEXAN-1-ONE-3β,4β-DICARBOXYLIC ACID ANHYDRIDE (Silane, [(3-methoxy-1-methylene-2-propenyl)oxy]trimethyl-) Preparation of Silane, [(3-methoxy-1-methylene-2-propenyl)oxy]trimethyl-. Submitted by Samuel Danishefsky, Takeshi Kitahara, and Paul F. Schuda1. DOI: 10.15227/orgsyn.061.0147. Organic Syntheses
PREPARATION AND DIELS-ALDER REACTION OF A REACTIVE, ELECTRON-DEFICIENT HETEROCYCLIC AZADIENE: DIMETHYL 1,2,4,5-TETRAZINE-3,6-DICARBOXYLATE. 1,2-DIAZINE (DIMETHYL 4-PHENYL-1,2-DIAZINE-3,6-DICARBOXYLATE) AND PYRROLE (DIMETHYL 3-PHENYLPYRROLE-2,5-DICARBOXYLATE) INTRODUCTION (1,2,4,5-Tetrazine-3,6-dicarboxylic acid, dimethyl ester; 3,6-Pyridazinedicarboxylic acid, 4-phenyl-, dimethyl ester; 1H-Pyrrole-2,5-dicarboxylic acid, 3-phenyl-, dimethyl ester) Preparation of 1,2,4,5-Tetrazine-3,6-dicarboxylic acid, dimethyl ester; 3,6-Pyridazinedicarboxylic acid, 4-phenyl-, dimethyl ester; 1H-Pyrrole-2,5-dicarboxylic acid, 3-phenyl-, dimethyl ester. Submitt… Organic Syntheses
PREPARATION AND INVERSE-ELECTRON-DEMAND DIELS–ALDER REACTION OF AN ELECTRON-DEFICIENT DIENE: METHYL 2-OXO-5,6,7,8-TETRAHYDRO-2H-1-BENZOPYRAN-3-CARBOXYLATE AND 6-METHOXY-7-METHOXYCARBONYL-1,2,3,4-TETRAHYDRONAPHTHALANE (2H-1-Benzopyran-3-carboxylic acid, 5, 6, 7, 8-tetrahydro-2-oxo-, methyl ester and 2-Naphthalenecarboxylic acid, 5, 6, 7, 8-tetrahydro-3-methoxy-, methyl ester) Preparation of 2H-1-Benzopyran-3-carboxylic acid, 5, 6, 7, 8-tetrahydro-2-oxo-, methyl ester and 2-Naphthalenecarboxylic acid, 5, 6, 7, 8-tetrahydro-3-methoxy-, methyl ester. Submitted by Dale L. Boge… Organic Syntheses
PREPARATION AND INVERSE-ELECTRON-DEMAND DIELS–ALDER REACTION OF AN ELECTRON-DEFICIENT HETEROCYCLIC AZADIENE: TRIETHYL 1,2,4-TRIAZINE-3,5,6-TRICARBOXYLATE AND 2,3,6-TRICARBOETHOXYPYRIDINE (1,2,4-Triazine-3,5,6-tricarboxylic acid, triethyl ester) Preparation of 1,2,4-Triazine-3,5,6-tricarboxylic acid, triethyl ester. Submitted by Dale L. Boger, James S. Panek, and Masami Yasuda1. DOI: 10.15227/orgsyn.066.0142. Organic Syntheses
PREPARATION AND REACTIONS OF 2-tert-BUTYL-1,1,3,3-TETRAMETHYLGUANIDINE: 2,2,6-TRIMETHYLCYCLOHEXEN-1-YL IODIDE Preparation of PREPARATION AND REACTIONS OF 2-tert-BUTYL-1,1,3,3-TETRAMETHYLGUANIDINE: 2,2,6-TRIMETHYLCYCLOHEXEN-1-YL IODIDE. Submitted by Derek H. R. Barton, Mi Chen, Joseph Cs. Jászberényi, and Denn… Organic Syntheses
PREPARATION AND REACTIONS OF ALKENYLCHROMIUM REAGENTS: 2-HEXYL-5-PHENYL-1-PENTEN-3-OL Preparation of PREPARATION AND REACTIONS OF ALKENYLCHROMIUM REAGENTS: 2-HEXYL-5-PHENYL-1-PENTEN-3-OL. Submitted by Kazuhiko Takai1, Koichi Sakogawa, Yasutaka Kataoka, Koichiro Oshima, and Kiitiro Utim… Organic Syntheses
PREPARATION AND REDUCTIVE CLEAVAGE OF ENOL PHOSPHATES: 5-METHYLCOPROST-3-ENE (Cholest-3-ene, 5-methyl-, (5β)-) Preparation of Cholest-3-ene, 5-methyl-, (5β)-. Submitted by D. C. Muchmore1. DOI: 10.15227/orgsyn.052.0109. Organic Syntheses
PREPARATION AND THREE-CARBON + TWO-CARBON CYCLOADDITION OF CYCLOPROPENONE 1,3-PROPANEDIOL KETAL: 5,5-DICYANO-4-PHENYL-2-CYCLOPENTEN-1-ONE 1,3-PROPANEDIOL KETAL (4,8-Dioxaspiro[2.5]oct-1-ene and 6,10-Dioxaspiro[4.5]dec-3-ene-1,1-dicarbonitrile, 2-phenyl-) Cycloaddition Preparation of 4,8-Dioxaspiro[2.5]oct-1-ene and 6,10-Dioxaspiro[4.5]dec-3-ene-1,1-dicarbonitrile, 2-phenyl-. Submitted by Dale L. Boger, Christine E. Brotherton, and Gunda I. Georg1. DOI: 10.15227/org… Organic Syntheses
PREPARATION AND USE OF A NEW DIFLUOROCARBENE REAGENT. TRIMETHYLSILYL 2-FLUOROSULFONYL-2,2-DIFLUOROACETATE: n-BUTYL 2,2-DIFLUOROCYCLOPROPANECARBOXYLATE ((Cyclopropanecarboxylic acid, 2,2-difluoro-, butyl ester and Acetic acid, difluoro(fluorosulfonyl)-, trimethylsilyl ester)) Preparation of (Cyclopropanecarboxylic acid, 2,2-difluoro-, butyl ester and Acetic acid, difluoro(fluorosulfonyl)-, trimethylsilyl ester). Submitted by W. R. Dolbier, Jr.1, F. Tian, J.-X. Duan, and Q.… Organic Syntheses
PREPARATION AND USE OF LITHIUM ACETYLIDE: 1-METHYL-2-ETHYNYL-endo-3,3-DIMETHYL-2-NORBORNANOL (Bicyclo[2.2.1]heptan-2-ol, 2-ethynyl-1,3,3-trimethyl-, (1R-endo)) Preparation of Bicyclo[2.2.1]heptan-2-ol, 2-ethynyl-1,3,3-trimethyl-, (1R-endo). Submitted by M. Mark Midland, Jim I. McLoughlin, and Ralph T. Werley Jr1. DOI: 10.15227/orgsyn.068.0014. Organic Syntheses
PREPARATION AND USE OF (METHOXYMETHOXY)METHYLLITHIUM: 1-(HYDROXYMETHYL)CYCLOHEPTANOL (Cycloheptanemethanol, 1-hydroxy-) Preparation of Cycloheptanemethanol, 1-hydroxy-. Submitted by Carl R. Johnson1, John R. Medich2, Rick L. Danheiser3, Karen R. Romines3, Hiroo Koyama3, and Stephen K. Gee3. DOI: 10.15227/orgsyn.071.014… Organic Syntheses
PREPARATION AND USE OF N,N'-DI-BOC-N"-TRIFLYLGUANIDINE (Carbamic acid, [[(trifluoromethyl)sulfonyl]carbonimidoyl]bis-, bis(1,1-dimethylethyl) ester) Preparation of Carbamic acid, [[(trifluoromethyl)sulfonyl]carbonimidoyl]bis-, bis(1,1-dimethylethyl) ester. Submitted by Tracy J. Baker, Mika Tomioka, and Murray Goodman1. DOI: 10.15227/orgsyn.078.009… Organic Syntheses
PREPARATION OF 1,4:5,8-DIMETHANO-1,2,3,4,5,6,7,8-OCTAHYDRO-9,10-DIMETHOXYANTHRACENIUM HEXACHLOROANTIMONATE (4+SbCl6−): A HIGHLY ROBUST RADICAL-CATION SALT (1,4:5,8-Dimethanoanthracene, 1,2,3,4,5,6,7,8-octahydro-9,10-dimethoxy-, radical ion(1+), hexachloroantimonate(1−)) Preparation of 1,4:5,8-Dimethanoanthracene, 1,2,3,4,5,6,7,8-octahydro-9,10-dimethoxy-, radical ion(1+), hexachloroantimonate(1−). Submitted by Rajendra Rathore1, Carrie L. Burns, and Mihaela I. Deseln… Organic Syntheses
Preparation of 1,5-Disubstituted 1,2,3-Triazoles via Ruthenium-catalyzed Azide Alkyne Cycloaddition Cycloaddition Preparation of Preparation of 1,5-Disubstituted 1,2,3-Triazoles via Ruthenium-catalyzed Azide Alkyne Cycloaddition. Submitted by James S. Oakdale and Valery V. Fokin1. DOI: 10.15227/orgsyn.090.0096. Organic Syntheses
Preparation of 1-Benzyl-2-methyl-3-(ethoxycarbonyl)-4-2-(phenylethyl)-1H-pyrrole from 4-Phenyl-1,2-butadiene Preparation of Preparation of 1-Benzyl-2-methyl-3-(ethoxycarbonyl)-4-2-(phenylethyl)-1H-pyrrole from 4-Phenyl-1,2-butadiene. Submitted by Shengjun Ni, Can Zhu, Jie Chen and Shengming Ma. *1. DOI: 10.1… Organic Syntheses
PREPARATION OF 1-BUTYL-3-METHYL IMIDAZOLIUM-BASED ROOM TEMPERATURE IONIC LIQUIDS (1H-Imidazolium, 1-butyl-3-methyl-, chloride (1−); 1H-Imidazolium, 1-butyl-3-methyl-, tetrafluoroborate (1−); 1H-Imidazolium, 1-butyl-3-methyl-, hexafluorophosphate (1−)) Preparation of 1H-Imidazolium, 1-butyl-3-methyl-, chloride (1−); 1H-Imidazolium, 1-butyl-3-methyl-, tetrafluoroborate (1−); 1H-Imidazolium, 1-butyl-3-methyl-, hexafluorophosphate (1−). Submitted by Ja… Organic Syntheses
PREPARATION OF 1-BUTYL-3-METHYLIMIDAZOLIUM TETRAFLUOROBORATE (1H-Imidazolium, 1-butyl-3-methyl, tetrafluoroborate (1−)) Preparation of 1H-Imidazolium, 1-butyl-3-methyl, tetrafluoroborate (1−). Submitted by Xavier Creary and Elizabeth D. Willis1. DOI: 10.15227/orgsyn.082.0166. Organic Syntheses
PREPARATION OF 1-METHOXY-2-(4-METHOXYPHENOXY)BENZENE (Benzene, 1-methoxy-2-(4-methoxyphenoxy)-) Preparation of Benzene, 1-methoxy-2-(4-methoxyphenoxy)-. Submitted by Elizabeth Buck and Zhiguo J. Song1. DOI: 10.15227/orgsyn.082.0069. Organic Syntheses
PREPARATION OF [1-(METHOXYMETHYLCARBAMOYL)ETHYL] PHOSPHONIC ACID BIS-(2,2,2-TRIFLUOROETHYL) ESTER: A USEFUL INTERMEDIATE IN THE SYNTHESIS OF Z-UNSATURATED N-METHOXY-N-METHYLAMIDES Preparation of PREPARATION OF [1-(METHOXYMETHYLCARBAMOYL)ETHYL] PHOSPHONIC ACID BIS-(2,2,2-TRIFLUOROETHYL) ESTER: A USEFUL INTERMEDIATE IN THE SYNTHESIS OF Z-UNSATURATED N-METHOXY-N-METHYLAMIDES. Subm… Organic Syntheses
Preparation of 1-Monoacylglycerols via the Suzuki-Miyaura Reaction: 2,3-Dihydroxypropyl (Z)-tetradec-7-enoate Cross-coupling Preparation of Preparation of 1-Monoacylglycerols via the Suzuki-Miyaura Reaction: 2,3-Dihydroxypropyl (Z)-tetradec-7-enoate. Submitted by Dexi Yang1, Valerie A. Cwynar1, David J. Hart1, Jakkam Madanm… Organic Syntheses
PREPARATION OF 1-[N-BENZYLOXYCARBONYL-(1S)-1-AMINO-2-OXOETHYL]-4-METHYL-2,6,7-TRIOXABICYCLO[2.2.2]OCTANE (Carbamic acid, [1-(4-methyl-2,6,7-trioxabicyclo[2.2.2]oct-1-yl)-2-oxoethyl]-, phenylmethyl ester, (S)-) Preparation of Carbamic acid, [1-(4-methyl-2,6,7-trioxabicyclo[2.2.2]oct-1-yl)-2-oxoethyl]-, phenylmethyl ester, (S)-. Submitted by Nicholas G. W. Rose, Mark A. Blaskovich, Ghotas Evindar, Scott Wilki… Organic Syntheses
PREPARATION OF 2,4-DISUBSTITUTED IMIDAZOLES: 4-(4-METHOXYPHENYL)-2-PHENYL-1H-IMIDAZOLE (1H-Imidazole, 4-(4-methoxyphenyl)-2-phenyl-) Preparation of 1H-Imidazole, 4-(4-methoxyphenyl)-2-phenyl-. Submitted by Bryan Li1, Charles K-F Chiu, Richard F. Hank, Jerry Murry, Joshua Roth, and Harry Tobiassen. DOI: 10.15227/orgsyn.081.0105. Organic Syntheses
PREPARATION OF 2-CHLORO-1,3-BIS(DIMETHYLAMINO)TRIMETHINIUM HEXAFLUOROPHOSPHATE ([Methanaminium, N-[2-chloro-3-(dimethylamino)-2-propenylidene]-N-methyl-, hexafluorophosphate(1-)]) Preparation of [Methanaminium, N-[2-chloro-3-(dimethylamino)-2-propenylidene]-N-methyl-, hexafluorophosphate(1-)]. Submitted by Ian W. Davies, Jean-Francois Marcoux, and Jeremy Taylor1. DOI: 10.15227/… Organic Syntheses
PREPARATION OF (3,5-DIMETHOXY-1-PHENYL-CYCLOHEXA-2,5-DIENYL)-ACETONITRILE THROUGH BIRCH REDUCTIVE ALKYLATION (BRA) Preparation of PREPARATION OF (3,5-DIMETHOXY-1-PHENYL-CYCLOHEXA-2,5-DIENYL)-ACETONITRILE THROUGH BIRCH REDUCTIVE ALKYLATION (BRA). Submitted by Raphaël Lebeuf, Muriel Berlande, Frédéric Robert, and Ya… Organic Syntheses
Preparation of 3-Alkylated Oxindoles from N-Benzyl Aniline via a Cu(II)-Mediated Anilide Cyclization Process Cyclization Preparation of Preparation of 3-Alkylated Oxindoles from N-Benzyl Aniline via a Cu(II)-Mediated Anilide Cyclization Process. Submitted by David S. Pugh1 and Richard J. K. Taylor1. DOI: 10.15227/orgsyn… Organic Syntheses
PREPARATION OF 3-BROMOPROPIOLIC ESTERS:METHYL AND tert-BUTYL 3-BROMOPROPIOLATES (2-Propynoic acid, 3-bromo-, methyl and 1,1-dimethylethyl esters) Preparation of 2-Propynoic acid, 3-bromo-, methyl and 1,1-dimethylethyl esters. Submitted by J. Leroy1. DOI: 10.15227/orgsyn.074.0212. Organic Syntheses
Preparation of 3-Oxocyclohex-1-ene-1-carbonitrile Preparation of Preparation of 3-Oxocyclohex-1-ene-1-carbonitrile. Submitted by Jesus Armando Lujan-Montelongo and Fraser F. Fleming.1. DOI: 10.15227/orgsyn.090.0229. Organic Syntheses
PREPARATION OF 4-ACETYLAMINO-2,2,6,6-TETRAMETHYLPIPERIDINE-1-OXOAMMONIUM TETRAFLUOROBORATE, AND THE OXIDATION OF GERANIOL TO GERANIAL (2,6-Octadienal, 3,7-dimethyl-, (2E)-) Oxidation Preparation of 2,6-Octadienal, 3,7-dimethyl-, (2E)-. Submitted by James M. Bobbitt and Nabyl Merbouh1. DOI: 10.15227/orgsyn.082.0080. Organic Syntheses
PREPARATION OF 4-ALKYL-AND 4-HALOBENZOYL CHLORIDES: 4-PENTYLBENZOYL CHLORIDE (Benzoyl chloride, 4-pentyl-) Preparation of Benzoyl chloride, 4-pentyl-. Submitted by Mary E. Neubert and D. L. Fishel1. DOI: 10.15227/orgsyn.061.0008. Organic Syntheses
PREPARATION OF 4-SPIROCYCLOHEXYLOXAZOLIDINONE BY C-H BOND NITRENE INSERTION (3-Oxa-1-azaspiro[4.5]decan-2-one) Preparation of 3-Oxa-1-azaspiro[4.5]decan-2-one. Submitted by Kim Huard and Hélène Lebel1. DOI: 10.15227/orgsyn.086.0059. Organic Syntheses
Preparation of 5-Hydroxycyclopentenones Via Conjugate Addition-Initiated Nazarov Cyclization Cyclization Preparation of Preparation of 5-Hydroxycyclopentenones Via Conjugate Addition-Initiated Nazarov Cyclization. Submitted by Joshua L. Brooks, Yu-Wen Huang, and Alison J. Frontier1*. DOI: 10.15227/orgsyn… Organic Syntheses
PREPARATION OF 9,10-DIMETHOXYPHENANTHRENE AND 3,6-DIACETYL-9,10-DIMETHOXYPHENANTHRENE ((Phenanthrene, 9,10-dimethoxy- and Ethanone, 1,1'-(9,10-dimethoxy-3,6-phenanthrenediyl)bis-)) Preparation of (Phenanthrene, 9,10-dimethoxy- and Ethanone, 1,1'-(9,10-dimethoxy-3,6-phenanthrenediyl)bis-). Submitted by Kamil Paruch, Libor Vyklicky, and Thomas J. Katz1. DOI: 10.15227/orgsyn.080.02… Organic Syntheses
PREPARATION OF A 1-ALKOXY-1-ALKYNE FROM REACTION OF A 2,2,2-TRIFLUOROMETHYL ETHER WITH AN ALKYLLITHIUM REAGENT (1-BENZYLOXYMETHOXY-1-HEXYNE) Preparation of 1-BENZYLOXYMETHOXY-1-HEXYNE. Submitted by P. J. Kocienski and T. N. Snaddon1. DOI: 10.15227/orgsyn.085.0045. Organic Syntheses
PREPARATION OF A CARBAZOLE-BASED MACROCYCLE VIA PRECIPITATION-DRIVEN ALKYNE METATHESIS Metathesis Preparation of PREPARATION OF A CARBAZOLE-BASED MACROCYCLE VIA PRECIPITATION-DRIVEN ALKYNE METATHESIS. Submitted by Wei Zhang, Hyeon Mo Cho, and Jeffrey S. Moore1. DOI: 10.15227/orgsyn.084.0177. Organic Syntheses
Preparation of Alkanesulfonyl Chlorides from S-Alkyl Isothiourea Salts via N-Chlorosuccinimide Mediated Oxidative Chlorosulfonation Preparation of Preparation of Alkanesulfonyl Chlorides from S-Alkyl Isothiourea Salts via N-Chlorosuccinimide Mediated Oxidative Chlorosulfonation. Submitted by Zhanhui Yang and Jiaxi Xu1*. DOI: 10.15… Organic Syntheses
PREPARATION OF A NON-SYMMETRICAL IMIDAZOLIUM SALT: 1-ADAMANTYL-3-MESITYL-4,5-DIMETHYLIMIDAZOLIUM TETRAFLUOROBORATE Preparation of PREPARATION OF A NON-SYMMETRICAL IMIDAZOLIUM SALT: 1-ADAMANTYL-3-MESITYL-4,5-DIMETHYLIMIDAZOLIUM TETRAFLUOROBORATE. Submitted by Alois Fürstner, Manuel Alcarazo, Vincent César, and Helg… Organic Syntheses
PREPARATION OF A TRIFLUOROMETHYL TRANSFER AGENT: 1-TRIFLUOROMETHYL-1,3-DIHYDRO-3,3-DIMETHYL-1,2-BENZIODOXOLE Preparation of PREPARATION OF A TRIFLUOROMETHYL TRANSFER AGENT: 1-TRIFLUOROMETHYL-1,3-DIHYDRO-3,3-DIMETHYL-1,2-BENZIODOXOLE. Submitted by Patrick Eisenberger, Iris Kieltsch, Raffael Koller, Kyrill Sta… Organic Syntheses
PREPARATION OF A TRISAMIDOMOLYBDENUM(VI) PROPYLIDYNE COMPLEX (− A HIGHLY ACTIVE CATALYST PRECURSOR FOR ALKYNE METATHESIS) Metathesis Preparation of − A HIGHLY ACTIVE CATALYST PRECURSOR FOR ALKYNE METATHESIS. Submitted by Wei Zhang, Yunyi Lu, and Jeffrey S. Moore1. DOI: 10.15227/orgsyn.084.0163. Organic Syntheses
PREPARATION OF BENZOCYCLOBUTENONE DERIVATIVES BASED ON AN EFFICIENT GENERATION OF BENZYNES (Bicyclo[4.2.0]octa-1,3,5-trien-7-one, 5-(phenylmethoxy)-) Preparation of Bicyclo[4.2.0]octa-1,3,5-trien-7-one, 5-(phenylmethoxy)-. Submitted by Shin-ichiro Tsujiyama and Keisuke Suzuki1a. DOI: 10.15227/orgsyn.084.0272. Organic Syntheses
PREPARATION OF BICYCLO[3.2.0]HEPT-3-EN-6-ONES: 1,4-DIMETHYLBICYCLO[3.2.0]HEPT-3-EN-6-ONE (Bicyclo[3.2.0]hept-3-en-6-one, 1,4-dimethyl-, cis-(±)-) Preparation of Bicyclo[3.2.0]hept-3-en-6-one, 1,4-dimethyl-, cis-(±)-. Submitted by Goffredo Rosini1, Giovanni Confalonieri2, Emanuela Marotta1, Franco Rama2, and Paolo Righi1. DOI: 10.15227/orgsyn.07… Organic Syntheses
PREPARATION OF BIS(2,4,6-TRIMETHYLPYRIDINE)IODINE(I) HEXAFLUOROPHOSPHATE AND BIS(2,4,6-TRIMETHYLPYRIDINE) BROMINE(I) HEXAFLUOROPHOSPHATE (Iodine(1+), bis(2,4,6-trimethylpyridine)-, hexafluorophosphate(1−), and Bromine(1+), bis(2,4,6-trimethylpyridine)-, hexafluorophosphate(1−)) Preparation of Iodine(1+), bis(2,4,6-trimethylpyridine)-, hexafluorophosphate(1−), and Bromine(1+), bis(2,4,6-trimethylpyridine)-, hexafluorophosphate(1−). Submitted by Fadi Homsi, Sylvie Robin, and G… Organic Syntheses
PREPARATION OF CHIRAL AND ACHIRAL TRIAZOLIUM SALTS: CARBENE PRECURSORS WITH DEMONSTRATED SYNTHETIC UTILITY Preparation of PREPARATION OF CHIRAL AND ACHIRAL TRIAZOLIUM SALTS: CARBENE PRECURSORS WITH DEMONSTRATED SYNTHETIC UTILITY. Submitted by Harit U. Vora, Stephen P. Lathrop, Nathan T. Reynolds, Mark S. K… Organic Syntheses
PREPARATION OF CHIRAL, NONRACEMIC γ-LACTONES BY ENZYMECATALYZED OXIDATION OF meso-DIOLS: ( + )-(1R,6S)-8-OXABICYCLO[4.3.0]NONAN-7-ONE (1(3H)-Isobenzofuranone, hexahydro-, (3aS-cis)-) Oxidation Preparation of 1(3H)-Isobenzofuranone, hexahydro-, (3aS-cis)-. Submitted by J. Bryan Jones and Ignac J. Jakovac1. DOI: 10.15227/orgsyn.063.0010. Organic Syntheses
PREPARATION OF CHLOROPHENYLDIAZIRINE AND THERMAL GENERATION OF CHLOROPHENYL CARBENE: 1,2-DIPHENYL-3-METHYLCYCLOPROPENE (Benzene, 1,1'-(3-methyl-1-cyclopropene-1,2-diyl)-bis-) Preparation of Benzene, 1,1'-(3-methyl-1-cyclopropene-1,2-diyl)-bis-. Submitted by Albert Padwa, Mitchell J. Pulwer, and Thomas J. Blacklock1. DOI: 10.15227/orgsyn.060.0053. Organic Syntheses
PREPARATION OF CYANOALKYNES: 3-PHENYL-2-PROPYNENITRILE (2-Propynenitrile, 3-phenyl-) Preparation of 2-Propynenitrile, 3-phenyl-. Submitted by Fen-Tair Luo, May-Wen Wang, and Ren-Tzong Wang1. DOI: 10.15227/orgsyn.075.0146. Organic Syntheses
PREPARATION OF CYANO COMPOUNDS USING ALKYLALUMINUM INTERMEDIATES: 1-CYANO-6-METHOXY-3,4-DIHYDRONAPHTHALENE (Naphthalenecarbonitrille, 3,4-dihydro-6-methoxy-) Preparation of Naphthalenecarbonitrille, 3,4-dihydro-6-methoxy-. Submitted by W. Nagata1, M. Yoshioka, and M. Murakami. DOI: 10.15227/orgsyn.052.0096. Organic Syntheses

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