Synthesis of polyynes by in situ desilylative bromination and palladium-catalyzed coupling: (7-(benzyloxy)hepta-1,3,5-triynyl)triisopropylsilane
Organic SynthesesCross-coupling
A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.
Reagents
| Compound | Role | Equiv | MW (g/mol) | ρ (g/mL) | Safety |
|---|---|---|---|---|---|
| Triisopropylsilane6459-79-6 | product | — | — | — | — |
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