Preparation of cycloheptane-1,3-dione via reductive ring expansion of 1-trimethylsilyloxy-7,7-dichlorobicyclo[3.2.0]heptan-6-one
CAS index name: Cycloheptane-1,3-dione
Organic Syntheses
A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.
Reagents
| Compound | Role | Equiv | MW (g/mol) | ρ (g/mL) | Safety |
|---|---|---|---|---|---|
| Cycloheptane-1,3-dione1194-18-9 · C7H10O2 | product | — | 126.16 | — | Warning |