Preparation of bis(2,4,6-trimethylpyridine)iodine(I) hexafluorophosphate and bis(2,4,6-trimethylpyridine) bromine(I) hexafluorophosphate

CAS index name: Iodine(1+), bis(2,4,6-trimethylpyridine)-, hexafluorophosphate(1−), and Bromine(1+), bis(2,4,6-trimethylpyridine)-, hexafluorophosphate(1−)

Organic Syntheses

Reaction scheme of Preparation of bis(2,4,6-trimethylpyridine)iodine(I) hexafluorophosphate and bis(2,4,6-trimethylpyridine) bromine(I) hexafluorophosphate from Organic Syntheses
Scheme as published in Org. Synth. Vol. 77, p. 206.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
2,4,6-Trimethylpyridine108-75-8 · C8H11N product — 121.18 0.910 Flammable (GHS02)Acute Toxic (GHS06)Irritant (GHS07)Danger

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