Preparation of bis(2,4,6-trimethylpyridine)iodine(I) hexafluorophosphate and bis(2,4,6-trimethylpyridine) bromine(I) hexafluorophosphate
CAS index name: Iodine(1+), bis(2,4,6-trimethylpyridine)-, hexafluorophosphate(1−), and Bromine(1+), bis(2,4,6-trimethylpyridine)-, hexafluorophosphate(1−)
Organic Syntheses

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.
Reagents
| Compound | Role | Equiv | MW (g/mol) | ρ (g/mL) | Safety |
|---|---|---|---|---|---|
| 2,4,6-Trimethylpyridine108-75-8 · C8H11N | product | — | 121.18 | 0.910 | Danger |