Synthesis of 4-(2-bromo-2-propenyl)-4-methyl-γ-butyrolactone by the reaction of ethyl levulinate with (2-bromoallyl)diisopropoxyborane prepared by haloboration of allene

CAS index name: 2(3H)-Furanone, 5-(2-bromo-2-propenyl)dihydro-5-methyl-

Organic Syntheses

Reaction scheme of Synthesis of 4-(2-bromo-2-propenyl)-4-methyl-γ-butyrolactone by the reaction of ethyl levulinate with (2-bromoallyl)diisopropoxyborane prepared by haloboration of allene from Organic Syntheses
Scheme as published in Org. Synth. Vol. 75, p. 129.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

The compound this preparation makes is not in the catalogue, so no reagents or figures are listed here.

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