Stereoselective alkene synthesis via 1-chloro-1-[(dimethyl)phenylsilyl]alkanes and α-(dimethyl)phenylsilyl ketones: 6-methyl-6-dodecene

Organic Syntheses

Reaction scheme of Stereoselective alkene synthesis via 1-chloro-1-[(dimethyl)phenylsilyl]alkanes and α-(dimethyl)phenylsilyl ketones: 6-methyl-6-dodecene from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 9, p. 580; Vol. 73, p. 50.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
Ethane74-84-0 · C2H6 product — 30.07 — Flammable (GHS02)Compressed Gas (GHS04)Danger

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