Methoxycarbonylmethylation of aldehydes via siloxycyclopropanes: methyl 3,3-dimethyl-4-oxobutanoate

CAS index name: Butanoic acid, 3,3-dimethyl-4-oxo-, methyl ester

Organic Syntheses

Reaction scheme of Methoxycarbonylmethylation of aldehydes via siloxycyclopropanes: methyl 3,3-dimethyl-4-oxobutanoate from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 9, p. 573; Vol. 71, p. 189.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

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