Double hydroxylation reaction for construction of the corticoid side chain: 16α-methylcortexolone

CAS index name: Pregn-4-ene-3,20-dione, 17,21-dihydroxy-16-methyl-, (16α)-(±)-

Organic Syntheses

Reaction scheme of Double hydroxylation reaction for construction of the corticoid side chain: 16α-methylcortexolone from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 9, p. 564; Vol. 73, p. 123.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

The compound this preparation makes is not in the catalogue, so no reagents or figures are listed here.

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