Inverse electron-demand Diels-Alder cycloaddition of a ketene dithioacetal. Copper hydride-promoted reduction of a conjugated enone. 9-Dithiolanobicyclo[3.2.2]non-6-en-2-one from tropone

Organic SynthesesCycloaddition

Reaction scheme of Inverse electron-demand Diels-Alder cycloaddition of a ketene dithioacetal. Copper hydride-promoted reduction of a conjugated enone. 9-Dithiolanobicyclo[3.2.2]non-6-en-2-one from tropone from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 9, p. 396; Vol. 71, p. 181.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

The compound this preparation makes is not in the catalogue, so no reagents or figures are listed here.

Named reactions in this procedure

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