Cyclopropanation using an iron-containing methylene transfer reagent: 1,1-diphenylcyclopropane

CAS index name: Iron (1+), dicarbonyl(η5-2,4-cyclopentadien-1-yl)(dimethylsulfonium η-methylide)-, tetrafluoroborate (1-) and Benzene, 1,1'-cyclopropylidenebis-

Organic Syntheses

Reaction scheme of Cyclopropanation using an iron-containing methylene transfer reagent: 1,1-diphenylcyclopropane from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 9, p. 372; Vol. 70, p. 177.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
1,1-Diphenylcyclopropane3282-18-6 · C15H14 product — 194.28 — —

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