(−)-(1S,4R)-CAMPHANOYL CHLORIDE (2-Oxabicyclo[2.2.1]heptane-1-carbonyl chloride, 4,7,7-trimethyl-3-oxo-, (1S)-))

Organic Syntheses

Procedure on orgsyn.org
Reaction scheme of (−)-(1S,4R)-CAMPHANOYL CHLORIDE (2-Oxabicyclo[2.2.1]heptane-1-carbonyl chloride, 4,7,7-trimethyl-3-oxo-, (1S)-)) from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 9, p. 151; Vol. 71, p. 48.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
3-Oxa-2-oxobornane-4-carbonyl chloride39637-74-6 · C10H13ClO3 product — 216.66 — Corrosive (GHS05)Danger

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Google Scholar PubMed Wikipedia DOI 10.15227/orgsyn.071.0048