Conversion of esters to allylsilanes: trimethyl(2-methylene-4-phenyl-3-butenyl)silane

CAS index name: Silane, trimethyl (2-methylene-4-phenyl-3-butenyl)-

Organic Syntheses

Procedure on orgsyn.org
Reaction scheme of Conversion of esters to allylsilanes: trimethyl(2-methylene-4-phenyl-3-butenyl)silane from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 8, p. 602; Vol. 69, p. 89.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
Trimethylsilane993-07-7 · C3H10Si product — 74.20 — Flammable (GHS02)Compressed Gas (GHS04)Irritant (GHS07)Danger

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Google Scholar PubMed Wikipedia DOI 10.15227/orgsyn.069.0089