Preparation and inverse-electron-demand Diels–Alder reaction of an electron-deficient heterocyclic azadiene: triethyl 1,2,4-triazine-3,5,6-tricarboxylate and 2,3,6-tricarboethoxypyridine

CAS index name: 1,2,4-Triazine-3,5,6-tricarboxylic acid, triethyl ester

Organic Syntheses

Reaction scheme of Preparation and inverse-electron-demand Diels–Alder reaction of an electron-deficient heterocyclic azadiene: triethyl 1,2,4-triazine-3,5,6-tricarboxylate and 2,3,6-tricarboethoxypyridine from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 8, p. 597; Vol. 66, p. 142.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

The compound this preparation makes is not in the catalogue, so no reagents or figures are listed here.

Named reactions in this procedure

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