Synthesis of alkyl propanoates by a haloform reaction of a trichloro ketone: ethyl 3,3-diethoxypropanoate

CAS index name: Propanoic acid, 3,3-diethoxy-, ethyl ester

Organic Syntheses

Reaction scheme of Synthesis of alkyl propanoates by a haloform reaction of a trichloro ketone: ethyl 3,3-diethoxypropanoate from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 8, p. 254; Vol. 69, p. 238.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
Ethyl 3,3-diethoxypropionate10601-80-6 · C9H18O4 product — 190.24 — Irritant (GHS07)Warning

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