Preparation and Diels–Alder reaction of a highly nucleophilic diene: trans-1-methoxy-3-trimethylsiloxy-1,3-butadiene and 5β-methoxycyclohexan-1-one-3β,4β-dicarboxylic acid anhydride
CAS index name: Silane, [(3-methoxy-1-methylene-2-propenyl)oxy]trimethyl-
Organic Syntheses
A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.
Reagents
| Compound | Role | Equiv | MW (g/mol) | ρ (g/mL) | Safety |
|---|---|---|---|---|---|
| [(3-Methoxy-1-methylene-2-propen-1-yl)oxy]trimethylsilane59414-23-2 · C8H16O2Si | product | — | 172.30 | — | — |