Synthesis of α,β-unsaturated nitriles from acetonitrile: cyclohexylideneacetonitrile and cinnamonitrile

CAS index name: Acetonitrile, cyclohexylidene- and 2-propenenitrile, 3-phenyl, (E)- and (Z)-

Organic Syntheses

Reaction scheme of Synthesis of α,β-unsaturated nitriles from acetonitrile: cyclohexylideneacetonitrile and cinnamonitrile from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 7, p. 108; Vol. 62, p. 179.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
Cinnamonitrile1885-38-7 · C9H7N product — 129.16 1.040 Acute Toxic (GHS06)Irritant (GHS07)Danger

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