Preparation of thiol esters: S-tert-butyl cyclohexanecarbothioate and S-tert-butyl 3α,7α,12α-trihydroxy-5β-cholane-24-thioate
CAS index name: Cyclohexanecarbothioic acid, S-(1,1-dimethylethyl)ester and cholane-24-thioic acid, 3,7,12-trihydroxy-S-(1,1-dimethylethyl)ester, (3α,5β,7α,12α)
Organic Syntheses
A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.
Reagents
The compound this preparation makes is not in the catalogue, so no reagents or figures are listed here.