Electrophilic N-amination of imide sodium salts with O-diphenylphosphinylhydroxylamine (DPH): 7-aminotheophylline

CAS index name: 1H-Purine-2,6-dione, 7-amino-3,7-dihydro-1,3-dimethyl-

Organic Syntheses

Reaction scheme of Electrophilic N-amination of imide sodium salts with O-diphenylphosphinylhydroxylamine (DPH): 7-aminotheophylline from Organic Syntheses
Scheme as published in Org. Synth. Coll. Vol. 7, p. 8; Vol. 64, p. 96.

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.

Reagents

CompoundRoleEquivMW (g/mol)ρ (g/mL)Safety
1,6-Diphenyl-1,3,5-hexatriene1720-32-7 · C18H16 product — 232.33 — —

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