Electrophilic N-amination of imide sodium salts with O-diphenylphosphinylhydroxylamine (DPH): 7-aminotheophylline
CAS index name: 1H-Purine-2,6-dione, 7-amino-3,7-dihydro-1,3-dimethyl-
Organic Syntheses

A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.
Reagents
| Compound | Role | Equiv | MW (g/mol) | ρ (g/mL) | Safety |
|---|---|---|---|---|---|
| 1,6-Diphenyl-1,3,5-hexatriene1720-32-7 · C18H16 | product | — | 232.33 | — | — |