Oxidation with the nitrosodisulfonate radical. I. Preparation and use of disodium nitrosodisulfonate: trimethyl-p-benzoquinone
CAS index name: Nitrosodisulfonic acid, disodium salt and 2,5-Cyclohexadiene-1,4-dione, 2,3,5-trimethyl-
Organic SynthesesOxidation
A checked procedure from Organic Syntheses, the journal whose preparations are repeated in a second laboratory before publication. The full experimental, with amounts, hazards and characterisation data, is on orgsyn.org.
Reagents
The compound this preparation makes is not in the catalogue, so no reagents or figures are listed here.
More oxidation reactions
- Air Oxidation of Primary Alcohols Catalyzed by Copper(I)/TEMPO. Preparation of 2-Amino-5-bromobenzaldehyde
- Aldehydes by oxidation of terminal olefins with chromyl chloride: 2,4,4-trimethylpentanal
- Aldehydes from primary alcohols by oxidation with chromium trioxide: heptanal
- Allylic Oxidation Catalyzed by Dirhodium(II) Tetrakis[ε-caprolactamate] of tert-Butyldimethylsilyl-protected trans-Dehydroandrosterone
- Allylic oxidation with hydrogen peroxide–selenium dioxide: trans-pinocarveol
- Anodic oxidation of acids: dimethyl decanedioate